If I calibrate my powder dropper for 3.2 grains, I am confident it won't drift more than 0.1 grain, plus or minus. But if I think I've calibrated it for 3.2 but the scales were off by 0.1, it could really be calibrated at 3.3 grains, and the drift could take it to 3.4, and the velocity goes outside my parameters. (or similarly for variations on the low end). That's assuming my OAL doesn't vary. If I get a slight setback it could add even more velocity
Any bullet setback is going to be a deal breaker with such tiny case volume.
One of Speer’s tests showed pressures more than double with a .030” difference in seating depth, in a larger 9mm case. Only going to get worse in a smaller case.
I have one Dillon powder bar that the last time it was adjusted was 2003 or 2004, it throws the same charge, to the tenth, every time I check it and amazingly even with many different lots of powders over the years.
However, you are not talking about accuracy or your measure but the ability of your scale to indicate an identical weight over time.
For this you just need a “standard”. It doesn’t have to be anything expensive or very fancy, all it needs to be is something that won’t change its mass over time and weigh close to what you are wanting to weigh.
For example, if you took a spent large primer, knocked the anvil out of it, cleaned out the residue and weighted it, you’ll be close to your target. Sand it a bit and you could get it right on your 3.2 grain target. Whatever it weighs when you are done is what it will weigh next month, next year, 5 years from now.
Now get a container you can’t lose, label it with the weight of the object you are going to keep inside it and keep it handy. If your scale says the object weighs different one time than it does others, I would trust the object didn’t change and your instrument is not telling you the truth.