After reading several of your posts over the last year or so about powder degrading I got rid of all my old powder yesterday. A pound of 2400, 3 or 4 pounds of 3031 in 1 lb cans and the remainder of a 8 pound cask of bullseye. These all dated back to 1980 at least, the 2400 was older as was the bullseye. The lawn thanks you and so do I. I did however keep the 2400 and bullseye cans, they are cool.
I am of the opinion that all gunpowders need to be inspected and sniff tested regularly. About once a year is probably fine. When gun hits a neutral smell, it is time to shoot it up. Every can of powder that went neutral for me, I started having storage issues, where the case necks would crack on loaded ammunition, firstly on being fired,
This was loaded with Pat's reloading surplus AA2520 and was in the case 10 years.
Same powder loaded in a 30-06 case for 13 years.
Might have been mid nineties AA4064. I am having all sorts of issues with this lot and am going to dump it out soon.
Get rid of gunpowder that shows this sort of deterioration:
This H5010, when poured out of the can, was glumpy
I consider this a dangerous level of deterioration and even if the chunks were broken to the point they flowed through a powder measure, I would not trust the stuff and would be concerned that it might blow up any firearm it was fired in.
I have some old ammo dates from the late 1940s, it still shoots just fine and Lord knows how that stuff was stored.
Ammunition that old, you are drinking alcohol , swallowing opiates and expecting nothing to happen. The greatest risk with that old stuff is that it might blow up your pistol. WW2 ammunition was never expected to have a 80 year shelf life and it was not manufactured with the expectation that it was going to be used decades forth.
There are lots of examples of younger ammunition that went bad. I recommend you pull some of those bullets and see if you have corrosion in the case.
This was estate sale ammunition, the boxes indicate 1950's ammunition. One case is showing pin hole corrosion from old gunpowder and when the bullet was pulled, corrosion on the bottom of the bullet. I would not shoot this stuff, I would pull the bullets, toss the cases, and toss the powder. I would toss the cases because I would fear the brass was deteriorated by exposure to nitric acid gas in the shell.
This is factory 1960's Norma 30-06. I sure as heck would pull the bullets and dump the rest.
Pull some bullets on your old ammunition and see if the bullets show corrosion.
Last month I disassembled some factory 30-06 of unknown vintage. I would say of the five or six cases, only one showed signs of deterioration. Bottom of that bullet was blackened and the inside of the case was dark. Some of the powder was red-brown. I kept the bullets. I just don't trust decades old ammunition given all the problems I have encountered with the stuff.
I am also not going to buy 1980's estate gun powder anymore. I have shot up cans that functioned perfectly, but you know, my hands, my eyes, my health are worth more than a bargain on old gunpowder. Basically I am not interested in gunpowders or ammunition more than 20 years old. I have shot cases of the stuff, and I have had plenty of pressure issues with old surplus ammunition. At the time I did not know why I was having high pressure indications, but now I know: pressures increase in old gunpowder. And old bulk gunpowder, that stuff will autocombust. I provided a link to a house fire above. Decades old gunpowder, if it is not outgassing or smell bitter, shoot it up immediately and get it out of the house.
The guys who took these pictures of their hoards of WW2 era gunpowder, they have no idea of the risk they are taking storing this stuff in their houses. Gunpowder does not get better with age, it gets more dangerous.