Ok, I found a posting in a Shiloh forum which I am reproducing exactly as it was posted there:
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the book is cast bullets by col e h harrison a publication by the national rifle assosiation.. c0py right 1979. reprinted from past articles of the american rifleman.. i think col e h harrison was the question and answer guy back then.. (these books have some really amazing stuff... )
question: it seems to me that cast bullets become harder upon standing, please explain.........
col harrison replies. your observasion is correct. lead alloys do harden considerbly for a time after casting (spontanious hardneing is ment here not that from heat treatment. ). this has had almost no mention in the cast bullet information and the misinformation published to handloaders for generations. it is remarkable that something which can greatly affect bullet performance. and which is observable and measurable with simple means., has been over looked so long.. the pracitcal considerations are extent of hardening which is 50% or more, and the time during which it takes effect. these are brought out in the foll0wing brinell harness meadurments made by the preceedure alread published in the american rifleman, on a bullet aloy at three day inetervals after casting... o means the day of casting.. o days+ brinell 13...3 days=brinell 14.5,,,6 days 15.5....9 days brinell 20,, ...12 days brinell 19....15 days brinnell 20.....18 days brinnell 19.5........ thus the alowy reached nearly its full hardness by the ninth day after casting, though it will continue to harden further very slowly for some time longer.. ... this takes pace in softer alloys also. these measurment were made on another bullet alloy at four day intervals after casting... 4 days 9.5,,,,,8 DYS BRINEELLL 10, 12 days brinell 12.5.........16 days BRINELL 13,,,, 20 days brinell 16... . the increase then nearly stopped. the meal thus reached almost full hardness by the 20th day. this may be a more usual time than the nine days of the other alloy. ..............
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On another forum site discussion on Lead alloys hardening with age, I saw:
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The wheelweights I work with (modern ones) air cool to about 8 and age in a fairly linear fashion to 12 in 7 days and then end up about 13 in a few weeks. If I add 2% tin to make 2.5/2.5 it ends up approaching 15.
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So, evidently, the hardening over a 2 or 3 week period can be pretty significant. For shooters using either cast or jacketed bullets at mid or high pressure loads, this is likely not a problem, as they prefer harder bullets to ensure no barrel leading. But for someone running low pressure cast bullet loads, and looking for better obturation, this appears to eb a significant issue. Another unexpected variable to try to control . . .
Jim G